Almaz Khalilov

Design and Construction of Distillation Column

Distillation column design preview

Overview

Detailed engineering analysis and design of a 40-plate distillation column for separating ethanol and p-xylene. Includes McCabe-Thiele analysis, tray hydraulics, column sizing, and safety considerations.

Distillation Column Design for Ethanol/P-xylene Separation

As part of my chemical engineering subject "Design and Construction of Equipment", I designed a distillation column to separate a mixture of ethanol and p-xylene. This project focused on applying distillation theory and engineering principles to a real-world separation problem.

Key Aspects

Key aspects of my work included:

  • Performing McCabe-Thiele analysis to determine the number of ideal and real stages required for separation
  • Calculating vapor and liquid flow rates throughout the column
  • Determining column diameter and tray spacing based on flooding considerations
  • Designing top and bottom trays, including detailed hydraulic calculations
  • Performing checks for entrainment, weeping, and pressure drop across trays
  • Sizing column internals such as downcomers and weirs
  • Selecting appropriate materials and determining shell thickness
  • Sizing and specifying nozzles for various stream entries and exits
  • Creating detailed equipment specification sheets and process flow diagrams
  • Addressing safety considerations and operational procedures for the distillation column

Skills Gained

Through this project, I gained practical experience in:

  • Applying distillation theory to complex separation processes
  • Performing iterative calculations to optimize column design
  • Using industry standards (TEMA, AS1210) to guide equipment design decisions
  • Considering safety and operational aspects in high-pressure, high-temperature processes
  • Developing comprehensive technical specifications for process equipment
  • Balancing theoretical ideals with practical design constraints
  • Creating 3D models of the distillation column and its components using Fusion 360
  • Developing 2D engineering drawings and layouts using AutoCAD
  • Utilizing Excel with macros for complex, iterative distillation calculations
  • Integrating software tools (Fusion 360, AutoCAD, Excel) to support and visualize the engineering design process

Figures and Renders

Full Column Design

Full distillation column front view

Front view of the complete 40-plate distillation column designed for ethanol/p-xylene separation

Distillation column plates view

Internal view showing the arrangement of all 40 sieve trays in the distillation column

Detailed Component Designs

Top plate detail

Detailed design of the top sieve tray with downcomers and weirs

Bottom plate detail

Detailed design of the bottom sieve tray with optimized hydraulic parameters

Column bottom assembly

Bottom section of the column showing the reboiler connection and base support structure

Process Diagrams & Calculations

Process flow diagram

Process flow diagram showing all streams, equipment connections and operating parameters

McCabe-Thiele diagram

McCabe-Thiele analysis used to determine theoretical stages and optimal feed location

Project Documentation

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